APPLICATION OF HIGH-PERFORMANCE THIN-LAYER CHROMATOGRAPHY FOR THE ECHINACEA PURPUREA IDENTIFICATION IN DIETARY SUPPLEMENTS AND MEDICINAL PRODUCTS BASED ON IT
DOI:
https://doi.org/10.30888/2663-5712.2024-27-00-005Keywords:
Echinacea purpurea, herb juice, root tincture, HPTLC, identification, dietary supplements, medicines.Abstract
Medicines and dietary supplements with Echinacea purpurea are presented in the pharmaceutical market of Ukraine. Various ingredients that are obtained from the rhizomes with roots or flowering parts of Echinacea are used in production. Often manufacturesMetrics
References
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Tang C., Guo T., Zhang Z., Yang P., Song H. Rapid visualized characterization of phenolic taste compounds in tea extract by high-performance thin-layer chromatography coupled to desorption electrospray ionization mass spectrometry. Food Chemistry. 2021. Vol. 355. P. 129555. doi: 10.1016/j.foodchem.2021.129555.
Moricz A., Ott P. Separation and detection of apricot leaf triterpenes by high-performance thin-layer chromatography combined with direct bioautography and mass spectrometry. Journal of Chromatography A. 2022. Vol. 1675. P. 463167. doi: 10.1016/j.chroma.2022.463167.
Domínguez-Rodríguez I., Plaza M., Marina, M. High-performance thin-layer chromatography and direct analysis in real time-high resolution mass spectrometry of non-extractable polyphenols from tropical fruit peels. Food Research International. 2021. Vol. 147. P. 110455. doi: 10.1016/j.foodres.2021.110455.
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Yadav K., Gupta T., Aeri V. High performance thin layer chromatography based chemo profiling of Ashvagandharishta and its antidepressant activity. Journal of Chromatography B. 2022. Vol. 1204. P. 123334. doi: 10.1016/j.jchromb.2022.123334.
Mulaudzi N., Combrinck S., Vermaak I., Joubert E., Viljoen A. High performance thin layer chromatography fingerprinting of rooibos (Aspalathus linearis) and honeybush (Cyclopia genistoides, Cyclopia intermedia and Cyclopia subternata) teas. Journal of Applied Research on Medicinal and Aromatic Plants. 2022. Vol. 30. P. 100378. doi: 10.1016/j.jarmap.2022.100378.
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Kravchenko K. V., Makeeva D. V., Tumkin I., Kalinichev S. V. Rapid analysis and classification of blue ballpoint pen inks using high-performance thin-layer chromatography and digital color analysis. Talanta. 2024. Vol. 275. P. 126117. doi: 10.1016/j.talanta.2024.126117.
Bergmann A. J., Breitenbach M., Munoz C., Simon E., McCombie G., Biedermann M., Schonborn A., Vermeirssen E. Towards detecting genotoxic chemicals in food packaging at thresholds of toxicological concern using bioassays with high-performance thin-layer chromatography. Food Packaging and Shelf Life. 2023. Vol. 36. P. 101052. doi: 10.1016/j.fpsl.2023.101052.
Attimarad M., Ahmed M., Aldhubaib B. E., Harsha S. High-performance thin layer chromatography: A powerful analytical technique in pharmaceutical drug discovery. Pharm Methods. 2011. Vol. 2, No. 2. P. 71-75. doi: 4103/2229-4708.84436.
Кoмпeндіум – лiкарські прeпaрaти. [Електронний ресурс]. – Режим доступу: https://compendium.com.ua/uk/bad/
Державний реєстр лікарських засобів України. [Електронний ресурс]. – Режим доступу: http://www.drlz.com.ua/ibp/ddsite.nsf/
Державна Фармакопея України: в 3 т. / Державне підприємство «Український науковий фармакопейний центр якості лікарських засобів». 2-е вид. Харків : Державне підприємство «Український науковий фармакопейний центр якості лікарських засобів», 2015. Т. 1. 1128. 360 с.
References
Asres, E., Layloff, T. and Ashenef, A. (2023) ‘Development and validation of a high-performance thin layer chromatography method for the simultaneous determination of amoxicillin and clavulanic acid combinations in tablet dosage forms’, Heliyon, 9(12), e22891. doi: https://doi.org/10.1016/j.heliyon.2023.e22891.
Tang, C. et al. (2021) ‘Rapid visualized characterization of phenolic taste compounds in tea extract by high-performance thin-layer chromatography coupled to desorption electrospray ionization mass spectrometry’, Food Chemistry, 355, 129555. doi: https://doi.org/10.1016/j.foodchem.2021.129555.
Moricz, A. and Ott, P. (2022) ‘Separation and detection of apricot leaf triterpenes by high-performance thin-layer chromatography combined with direct bioautography and mass spectrometry’, Journal of Chromatography A, 1675, 463167. doi: https://doi.org/10.1016/j.chroma.2022.463167.
Domínguez-Rodríguez, I., Plaza, M. and Marina, M. (2021) ‘High-performance thin-layer chromatography and direct analysis in real time-high resolution mass spectrometry of non-extractable polyphenols from tropical fruit peels’, Food Research International, 147, 110455. doi: https://doi.org/10.1016/j.foodres.2021.110455.
Radosavljevic-Stevanovic, N. et al. (2023) ‘High-Performance Thin-Layer Chromatography hyphenated with image processing and chemometrics as a tool for forensic discrimination of Cannabis sativa L. chemotypes’, Forensic Chemistry, 36, 100528. doi: https://doi.org/10.1016/j.forc.2023.100528
Antunes, K. A. et al. (2024) ‘Comprehensive high-performance thin-layer chromatography analysis of Monteverdia ilicifolia leaf and its adulterants’, Natural Product Research, pp. 1-6. doi: https://doi.org/10.1080/14786419.2023.2289080.
Baglyas, M. et al. (2022) ‘High-performance thin-layer chromatography – antibacterial assay first reveals bioactive clerodane diterpenes in giant goldenrod (Solidago gigantea Ait.)’, Journal of Chromatography A, 1677, 463308. doi: https://doi.org/10.1016/j.chroma.2022.463308.
Yadav, K., Gupta, T. and Aeri, V. (2022) ‘High performance thin layer chromatography based chemo profiling of Ashvagandharishta and its antidepressant activity’, Journal of Chromatography B, 1204, 123334. doi: https://doi.org/10.1016/j.jchromb.2022.123334.
Mulaudzi, N. et al. (2022) ‘High performance thin layer chromatography fingerprinting of rooibos (Aspalathus linearis) and honeybush (Cyclopia genistoides, Cyclopia intermedia and Cyclopia subternata) teas’, Journal of Applied Research on Medicinal and Aromatic Plants, 30, 100378. doi: https://doi.org/10.1016/j.jarmap.2022.100378.
Kochale, K. et al. (2024) ‘Online coupling of miniaturized HPLC and high performance thin layer chromatography by a fractionation unit for effect directed analysis’, Advances in Sample Preparation, 9, 100102. doi: https://doi.org/10.1016/j.sampre.2024.100102.
Kravchenko, A.V. et al. (2024) ‘Rapid analysis and classification of blue ballpoint pen inks using high-performance thin-layer chromatography and digital color analysis’, Talanta, 275, 126117. doi: https://doi.org/10.1016/j.talanta.2024.126117.
Bergmann, A. J. et al. (2023) ‘Towards detecting genotoxic chemicals in food packaging at thresholds of toxicological concern using bioassays with high-performance thin-layer chromatography’, Food Packaging and Shelf Life, 36, 101052. doi: https://doi.org/10.1016/j.fpsl.2023.101052 .
Attimarad, M. et al. (2011) ‘High-performance thin layer chromatography: A powerful analytical technique in pharmaceutical drug discovery’, Pharm Methods, 2(2), pp. 71-75. doi: https://doi.org/10.4103/2229-4708.84436.
Кoмпeндіум – лiкарські прeпaрaти. Available at: https://compendium.com.ua/uk/bad/ (Accessed: 26 April 2024).
Державний реєстр лікарських засобів України. Available at: http://www.drlz.com.ua/ibp/ddsite.nsf/ (Accessed: 26 April 2024).
Державна Фармакопея України, (2016) ДП «Український науковий фармакопейний центр якості лікарських засобів». 2-е вид., доп. 1. Харків: Держ. п-во «Український науковий фармакопейний центр якості лікарських засобів», 360 с.
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